Technology Process of C23H24N4O6
There total 6 articles about C23H24N4O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonia / ethanol; water / 22 h / 20 °C / pH 8 - 9 / Inert atmosphere
2: sodium hydroxide / water / 0 °C / pH 12 - 13 / Inert atmosphere
3: N,N-dimethyl-formamide / 20 °C / Inert atmosphere
With
ammonia; sodium hydroxide;
In
ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100404
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / water / 0 °C / pH 12 - 13 / Inert atmosphere
2: N,N-dimethyl-formamide / 20 °C / Inert atmosphere
With
sodium hydroxide;
In
water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100404
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C / Inert atmosphere
2: silver(l) oxide / N,N-dimethyl-formamide / 5 - 20 °C / Inert atmosphere
3: hydrogenchloride / ester / -10 - -5 °C / Inert atmosphere; Cooling with ice
4: ammonia / ethanol; water / 22 h / 20 °C / pH 8 - 9 / Inert atmosphere
5: sodium hydroxide / water / 0 °C / pH 12 - 13 / Inert atmosphere
6: N,N-dimethyl-formamide / 20 °C / Inert atmosphere
With
pyridine; hydrogenchloride; ammonia; trifluoroacetic anhydride; sodium hydroxide; silver(l) oxide;
In
ester; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100404
