Technology Process of C50H67N7O9
There total 7 articles about C50H67N7O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C46H61N5O7;
With
hydrogenchloride; water;
In
1,4-dioxane;
at 20 ℃;
for 2.5h;
Inert atmosphere;
N-methoxycarbonyl-L-valine;
With
4-methyl-morpholine; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
1,4-dioxane; N,N-dimethyl-formamide;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/jm401398x
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: platinum(IV) oxide; hydrogen / tetrahydrofuran; ethanol / 0.5 h / 20 °C / 1551.49 Torr / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere
3.1: hydrogenchloride; water / 1,4-dioxane / 2.5 h / 20 °C / Inert atmosphere
3.2: 4 h / 20 °C / Inert atmosphere
With
hydrogenchloride; platinum(IV) oxide; water; hydrogen; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dimethyl sulfoxide;
DOI:10.1021/jm401398x
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere
2.1: hydrogenchloride; water / 1,4-dioxane / 2.5 h / 20 °C / Inert atmosphere
2.2: 4 h / 20 °C / Inert atmosphere
With
hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,4-dioxane; dimethyl sulfoxide;
DOI:10.1021/jm401398x