C₁₉H₂₉N₄O₆P

Base Information

• Chemical Name: C₁₉H₂₉N₄O₆P
• CAS No.: 1372791-22-4
• Molecular Formula: C₁₉H₂₉N₄O₆P
• Molecular Weight: 440.436
• Mol file: 1372791-22-4.mol

Synonyms:

Chemical Property of C₁₉H₂₉N₄O₆P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₉N₄O₆P

There total 5 articles about C₁₉H₂₉N₄O₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl N-[4-(2-bromoacetyl)phenyl]carbamate (885269-70-5) → C19H29N4O6P (1372791-22-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 3 h / 160 °C

2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane / 36 h / Reflux

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane;

DOI:10.1021/ja301868p

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → C19H29N4O6P (1372791-22-4)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium carbonate

2: aluminum (III) chloride; bromine / tetrahydrofuran

3: 3 h / 160 °C

4: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane / 36 h / Reflux

With aluminum (III) chloride; bromine; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; sodium hydroxide; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja301868p

Reference yield:

tert-butyl 4-acetylphenylcarbamate (232597-42-1) → C19H29N4O6P (1372791-22-4)

Guidance literature:

Multi-step reaction with 3 steps

1: aluminum (III) chloride; bromine / tetrahydrofuran

2: 3 h / 160 °C

3: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane / 36 h / Reflux

With aluminum (III) chloride; bromine; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja301868p

upstream raw materials:

tert-butyl N-[4-(2-bromoacetyl)phenyl]carbamate

1-azido-2-iodoethane

di-tert-butyl dicarbonate

p-aminobenzophenone

Downstream raw materials:

C₂₇H₃₃N₃O₄

(E)-4-(4-(4-aminobenzylidene)-3,4-dihydro-2H-pyrrol-5-yl)aniline

(E)-2-chloro-N-(4-(4-(4-(2-chloroacetamido)benzylidene)-3,4-dihydro-2H-pyrrol-5-yl)phenyl)acetamide