PdCl(CH₃)((CH₃)2C₃HN₂)2CHCH₂C₆H₅

Base Information

• Chemical Name: PdCl(CH₃)((CH₃)2C₃HN₂)2CHCH₂C₆H₅
• CAS No.: 1234862-25-9
• Molecular Formula: C₁₉H₂₅ClN₄Pd
• Molecular Weight: 451.307

Synonyms:

Chemical Property of PdCl(CH₃)((CH₃)2C₃HN₂)2CHCH₂C₆H₅

Chemical Property:

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Technology Process of PdCl(CH₃)((CH₃)2C₃HN₂)2CHCH₂C₆H₅

There total 1 articles about PdCl(CH₃)((CH₃)2C₃HN₂)2CHCH₂C₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-phenyl-2,2-bis(3,5-dimethylpyrazol-1-yl)ethane (918794-23-7) + chloromethyl(1,5-cyclooctadiene)palladium(II) → PdCl(CH3)((CH3)2C3HN2)2CHCH2C6H5 (1234862-25-9)

Guidance literature:

In diethyl ether; byproducts: C8H12; (Ar), Et2O added to Pd complex and ligand (1:1) at room temp., stirred overnight; evapd.(vac.), washed (pentane), elem. anal.;

DOI:10.1002/ejic.200900869

Reference yield: 94.0%

PdCl(CH3)((CH3)2C3HN2)2CHCH2C6H5 (1234862-25-9) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) + acetonitrile (75-05-8,26809-02-9) → Pd(CH3CN)(CH3)((CH3)2C3HN2)2CHCH2C6H5(1+)*B((CF3)2C6H3)4(1-)=Pd(CH3CN)CH3((CH3)2C3HN2)2CHCH2C6H5B((CF3)2C6H3)4 (1234862-30-6)

Guidance literature:

In dichloromethane; byproducts: NaCl; (Ar), 1 equiv. of Na(BArF)4 added to soln. of Pd complex in CH2Cl2 in the presence of excess CH3CN, stirred at room temp. for 1 h; NaCl filtered off, evapd.(vac.), washed (pentane), elem. anal.;

DOI:10.1002/ejic.200900869

upstream raw materials:

1-phenyl-2,2-bis(3,5-dimethylpyrazol-1-yl)ethane

Downstream raw materials:

Pd(CH₃CN)(CH₃)((CH₃)2C₃HN₂)2CHCH₂C₆H₅⁽¹⁺⁾*B((CF₃)2C₆H₃)4^(1-)=Pd(CH₃CN)CH₃((CH₃)2C₃HN₂)2CHCH₂C₆H₅B((CF₃)2C₆H₃)4

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