Technology Process of C15H15Cl2N5O
There total 10 articles about C15H15Cl2N5O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: copper / dimethyl sulfoxide
2: sodium hydroxide; water
3: oxalyl dichloride / N,N-dimethyl-formamide; hexane / 1 h / 20 °C
4: ammonia / water
5: trifluoroacetic anhydride
6: sodium hydride / tetrahydrofuran
7: hydrazine hydrate / ethanol
8: 8 h / 160 - 180 °C
9: potassium carbonate / N,N-dimethyl-formamide
10: sodium tetrahydroborate / methanol
With
sodium tetrahydroborate; oxalyl dichloride; ammonia; water; copper; sodium hydride; potassium carbonate; hydrazine hydrate; trifluoroacetic anhydride; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm4001314
- Guidance literature:
-
Multi-step reaction with 7 steps
1: ammonia / water
2: trifluoroacetic anhydride
3: sodium hydride / tetrahydrofuran
4: hydrazine hydrate / ethanol
5: 8 h / 160 - 180 °C
6: potassium carbonate / N,N-dimethyl-formamide
7: sodium tetrahydroborate / methanol
With
sodium tetrahydroborate; ammonia; sodium hydride; potassium carbonate; hydrazine hydrate; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm4001314
- Guidance literature:
-
Multi-step reaction with 6 steps
1: trifluoroacetic anhydride
2: sodium hydride / tetrahydrofuran
3: hydrazine hydrate / ethanol
4: 8 h / 160 - 180 °C
5: potassium carbonate / N,N-dimethyl-formamide
6: sodium tetrahydroborate / methanol
With
sodium tetrahydroborate; sodium hydride; potassium carbonate; hydrazine hydrate; trifluoroacetic anhydride;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm4001314