C₃₃H₅₆N₄O₈Si

Base Information

• Chemical Name: C₃₃H₅₆N₄O₈Si
• CAS No.: 1426655-86-8
• Molecular Formula: C₃₃H₅₆N₄O₈Si
• Molecular Weight: 664.915
• Mol file: 1426655-86-8.mol

Synonyms:

Chemical Property of C₃₃H₅₆N₄O₈Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₅₆N₄O₈Si

There total 15 articles about C₃₃H₅₆N₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H19NO3*ClH (1426656-15-6) + C20H39N3O6Si (1426656-79-2) → C33H56N4O8Si (1426655-86-8)

Guidance literature:

C₂₀H₃₉N₃O₆Si; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -20 ℃; for 1h; Inert atmosphere;

C₁₃H₁₉NO₃*ClH; With 4-methyl-morpholine; In tetrahydrofuran; at -20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c3cc00178d

Reference yield:

C34H61N3O7Si2 (1426656-67-8) → C33H56N4O8Si (1426655-86-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: (1S)-10-camphorsulfonic acid / dichloromethane; methanol / 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium periodate; rhodium(III) chloride hydrate / acetonitrile; water; acetone / 2 h / 20 - 25 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / Inert atmosphere

4.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere

4.2: 2 h / -20 °C / Inert atmosphere

With 4-methyl-morpholine; sodium periodate; rhodium(III) chloride hydrate; palladium 10% on activated carbon; (1S)-10-camphorsulfonic acid; hydrogen; isobutyl chloroformate; In tetrahydrofuran; methanol; dichloromethane; water; acetone; acetonitrile;

DOI:10.1039/c3cc00178d

Reference yield:

C21H25NO5 (1426657-14-8) → C33H56N4O8Si (1426655-86-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen; hydrogenchloride / methanol / 14 h / 20 °C / Inert atmosphere

2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere

2.2: 2 h / -20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; isobutyl chloroformate; In tetrahydrofuran; methanol;

DOI:10.1039/c3cc00178d

upstream raw materials:

C₃₄H₆₁N₃O₇Si₂

C₂₈H₄₇N₃O₇Si

C₂₈H₄₅N₃O₈Si

benzyl (2S,3S,4S)-3-hydroxy-5-[(S)-4-isopropyl-2-oxooxazolidin-3-yl]-4-methyl-5-oxo-1-phenylpentan-2-ylcarbamate

Downstream raw materials:

C₃₇H₆₁N₇O₉Si

actinoramide A

C₃₇H₆₀N₆O₉Si

padanamide B