Technology Process of C17H13Cl2NOS
There total 6 articles about C17H13Cl2NOS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium methylate / butan-1-ol / 15 h / 140 °C
2: phosphorus pentachloride / dichloromethane / 4 h / Reflux
3: ammonium hydroxide / acetone / 0.5 h / 0 - 15 °C
4: tetraphosphorus decasulfide / tetrahydrofuran / 4 h / 50 - 55 °C
5: 3 h / Reflux
With
ammonium hydroxide; tetraphosphorus decasulfide; phosphorus pentachloride; sodium methylate;
In
tetrahydrofuran; dichloromethane; acetone; butan-1-ol;
DOI:10.1007/s00044-012-0195-7
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium methylate / butan-1-ol / 15 h / 140 °C
2: phosphorus pentachloride / dichloromethane / 4 h / Reflux
3: ammonium hydroxide / acetone / 0.5 h / 0 - 15 °C
4: tetraphosphorus decasulfide / tetrahydrofuran / 4 h / 50 - 55 °C
5: 3 h / Reflux
With
ammonium hydroxide; tetraphosphorus decasulfide; phosphorus pentachloride; sodium methylate;
In
tetrahydrofuran; dichloromethane; acetone; butan-1-ol;
DOI:10.1007/s00044-012-0195-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: phosphorus pentachloride / dichloromethane / 4 h / Reflux
2: ammonium hydroxide / acetone / 0.5 h / 0 - 15 °C
3: tetraphosphorus decasulfide / tetrahydrofuran / 4 h / 50 - 55 °C
4: 3 h / Reflux
With
ammonium hydroxide; tetraphosphorus decasulfide; phosphorus pentachloride;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1007/s00044-012-0195-7
