[Tl(((2,6-difluorophenyl)NC(Me))2CH)]

Base Information

• Chemical Name: [Tl(((2,6-difluorophenyl)NC(Me))2CH)]
• CAS No.: 946532-01-0
• Molecular Formula: C₁₇H₁₃F₄N₂*Tl
• Molecular Weight: 525.68

Synonyms:

Chemical Property of [Tl(((2,6-difluorophenyl)NC(Me))2CH)]

Chemical Property:

Purity/Quality:

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Technology Process of [Tl(((2,6-difluorophenyl)NC(Me))2CH)]

There total 1 articles about [Tl(((2,6-difluorophenyl)NC(Me))2CH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

thallium(I) acetate (563-68-8) → [Tl(((2,6-difluorophenyl)NC(Me))2CH)] (946532-01-0)

Guidance literature:

In tetrahydrofuran; (N2); using Schlenk techniques; charging flask with Li(((2,6-difluorophenyl)NC(Me))2CH) and THF; addn. of Tl(OAc); stirring in the dark for 24 hat room temp.; removal of all volatiles in vac., extn. into Et2O; filtration, concn. invac., crystn. at -25°C for several ds; filtration, drying in vac .;

DOI:10.1021/om7003207

Reference yield: 79.0%

Mo(N-2,6-i-Pr2C6H3)(CHCMe2Ph)(OTf)2(DME) (645391-49-7) + [Tl(((2,6-difluorophenyl)NC(Me))2CH)] (946532-01-0) → [Mo(2,6-diisopropylphenylimido)(neophylidene)(((2,6-difluorophenyl)NC(Me))2CH)(trifluoromethanesulfonato)]

Guidance literature:

In toluene; byproducts: thallium trifluoromethanesulfonate, DME; (N2); using Schlenk techniques; charging of soln. of Mo(N(2,6-i-Pr2C6H3))(CHCMe2Ph)(OTf)2(DME) in toluene in flask; addn. of Tl(((3,5-dichlorophenyl)NC(Me))2CH); stirring at room temp. for 40 h; removal of all volatiles in vac., extn. into toluene; filtration, evapn.to dryness; dissolving in min. amt. of Et2O; crystn. at -25°C; p ptn.; as mixt. of syn and anti isomers; elem. anal.;

DOI:10.1021/om7003207

upstream raw materials:

thallium(I) acetate

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