C₂₃H₂₆N₆O₃

Base Information

• Chemical Name: C₂₃H₂₆N₆O₃
• CAS No.: 1610766-88-5
• Molecular Formula: C₂₃H₂₆N₆O₃
• Molecular Weight: 434.498
• Mol file: 1610766-88-5.mol

Synonyms:

Chemical Property of C₂₃H₂₆N₆O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₆N₆O₃

There total 12 articles about C₂₃H₂₆N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(1-azidoethyl)-3-nitrobenzene (246240-16-4) → C23H26N6O3 (1610766-88-5)

Guidance literature:

Multi-step reaction with 5 steps

1.1: triphenylphosphine / tetrahydrofuran; water / Inert atmosphere

2.1: D-tartaric acid / methanol / Inert atmosphere

2.2: Inert atmosphere

3.1: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / Inert atmosphere

4.1: ethyl acetate / 20 °C / Inert atmosphere

5.1: dichloromethane / 0 - 20 °C / Inert atmosphere

With D-tartaric acid; 10 wt% Pd(OH)2 on carbon; hydrogen; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate;

DOI:10.3109/14756366.2013.793184

Reference yield:

3-Nitroacetophenone (121-89-1) → C23H26N6O3 (1610766-88-5)

Guidance literature:

Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

2.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / Inert atmosphere

3.1: triphenylphosphine / tetrahydrofuran; water / Inert atmosphere

4.1: D-tartaric acid / methanol / Inert atmosphere

4.2: Inert atmosphere

5.1: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / Inert atmosphere

6.1: ethyl acetate / 20 °C / Inert atmosphere

7.1: dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; D-tartaric acid; diphenyl phosphoryl azide; 10 wt% Pd(OH)2 on carbon; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; toluene;

DOI:10.3109/14756366.2013.793184

Reference yield:

3-nitro-α-methylbenzylamine (90271-37-7,297730-25-7) → C23H26N6O3 (1610766-88-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: D-tartaric acid / methanol / Inert atmosphere

1.2: Inert atmosphere

2.1: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol / Inert atmosphere

3.1: ethyl acetate / 20 °C / Inert atmosphere

4.1: dichloromethane / 0 - 20 °C / Inert atmosphere

With D-tartaric acid; 10 wt% Pd(OH)2 on carbon; hydrogen; In methanol; ethanol; dichloromethane; ethyl acetate;

DOI:10.3109/14756366.2013.793184

upstream raw materials:

C₉H₇N₃O

C₁₄H₁₉N₃O₂

3-Nitroacetophenone

1-(1-azidoethyl)-3-nitrobenzene