1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene

Base Information

Chemical Name:1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene
CAS No.:205180-67-2
Molecular Formula:C₁₆H₁₄Br₂N₂O₂S₂
Molecular Weight:490.239
Hs Code.:

Synonyms:

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Chemical Property of 1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene

Chemical Property:

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Technology Process of 1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene

There total 5 articles about 1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82002-59-3
o-phenylenedioxydi-acetic acid diamide

: 205180-67-2
1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / Lawesson's reagent / tetrahydrofuran / Heating

2: 80 percent / ethanol / 7 h / Heating

3: 98 percent / LiAlH₄ / tetrahydrofuran / 2 h

4: Et₃N / CH₂Cl₂ / 0.5 h

5: LiBr / CH₂Cl₂; acetone / 1 h / Ambient temperature

With Lawessons reagent; lithium aluminium tetrahydride; triethylamine; lithium bromide; In tetrahydrofuran; ethanol; dichloromethane; acetone;
DOI:10.1002/jhet.5570350134

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 205180-67-2
1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene

Guidance literature:: Multi-step reaction with 6 steps

1: 76 percent / K₂CO₃ / acetone / 5 h / Heating

2: 70 percent / Lawesson's reagent / tetrahydrofuran / Heating

3: 80 percent / ethanol / 7 h / Heating

4: 98 percent / LiAlH₄ / tetrahydrofuran / 2 h

5: Et₃N / CH₂Cl₂ / 0.5 h

6: LiBr / CH₂Cl₂; acetone / 1 h / Ambient temperature

With Lawessons reagent; lithium aluminium tetrahydride; potassium carbonate; triethylamine; lithium bromide; In tetrahydrofuran; ethanol; dichloromethane; acetone;
DOI:10.1002/jhet.5570350134

Reference yield:

: 205180-60-5
1,2-bis(thioamidomethyloxy)benzene

: 205180-67-2
1,2-bis[2'(4'-bromomethyl)thiazolyl]methyloxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / ethanol / 7 h / Heating

2: 98 percent / LiAlH₄ / tetrahydrofuran / 2 h

3: Et₃N / CH₂Cl₂ / 0.5 h

4: LiBr / CH₂Cl₂; acetone / 1 h / Ambient temperature

With lithium aluminium tetrahydride; triethylamine; lithium bromide; In tetrahydrofuran; ethanol; dichloromethane; acetone;
DOI:10.1002/jhet.5570350134