Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2

Base Information

Chemical Name:Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2
CAS No.:15712-31-9
Molecular Formula:C₄₂H₃₅O₅P₂Tc
Molecular Weight:779.592
Hs Code.:

Tc(CO)3(C(O)OC<sub>2</sub>H<sub>5</sub>)(P(C<sub>6</sub>H<sub>5</sub>)3)2

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Chemical Property of Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2

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Technology Process of Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2

There total 2 articles about Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 64-17-5
ethanol

: 15747-04-3
Tc(CO)3(C(O)OCH₃)(P(C₆H₅)3)2

: 15712-31-9
Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2

Guidance literature:: In acetone; N2-atmosphere; stirring Tc-complex with 1 equiv. EtOH for 24 h; pptn. on concn., filtration, washing (Et2O), drying (vac.);
DOI:10.1016/0022-328X(95)05695-L

Reference yield: 59.0%

: 64-17-5
ethanol

: trans-[Tc(CO)4(PPh₃)2]BF₄

: 15712-31-9
Tc(CO)3(C(O)OC₂H₅)(P(C₆H₅)3)2

Guidance literature:: With sodium hydroxide; In ethanol; N2-atmosphere; addn. of 1 M NaOH to Tc-complex soln., stirring for 8 h; filtration, washing (Et2O), drying (vac.); elem. anal.;
DOI:10.1016/0022-328X(95)05695-L