N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide

Base Information

Chemical Name:N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide
CAS No.:1286315-73-8
Molecular Formula:C₂₄H₂₅N₂O₃*I
Molecular Weight:516.379
Hs Code.:

Synonyms:

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Chemical Property of N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide

Chemical Property:

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Technology Process of N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide

There total 4 articles about N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1286315-72-7
N-[(3-(dimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide

: 74-88-4
methyl iodide

: 1286315-73-8
N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide

Guidance literature:: In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo102531f

Reference yield:

: 1286315-71-6
2-[2-(4-hydroxyphenyl)ethyl]-1H-benz[de]isoquinoline-1,3(2H)-dione

: 1286315-73-8
N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / toluene / 4 h / Inert atmosphere; Reflux

2: acetonitrile / 20 °C / Inert atmosphere

With potassium carbonate; In toluene; acetonitrile; 1: Mannich reaction;
DOI:10.1021/jo102531f

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1286315-73-8
N-[(3-(trimethylamino)methyl-4-hydroxyphenyl)ethyl]-1,8-naphthalimide iodide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 1 h / 130 °C / Microwave irradiation

2: potassium carbonate / toluene / 4 h / Inert atmosphere; Reflux

3: acetonitrile / 20 °C / Inert atmosphere

With pyridine; potassium carbonate; In toluene; acetonitrile; 2: Mannich reaction;
DOI:10.1021/jo102531f