1-[4-(3-dimethylammoniumpropoxy)phenyl]-1-(4-hydroxyphenyl)-2-ferrocenyl-but-1-ene citrate

Base Information

• Chemical Name: 1-[4-(3-dimethylammoniumpropoxy)phenyl]-1-(4-hydroxyphenyl)-2-ferrocenyl-but-1-ene citrate
• CAS No.: 1291080-42-6
• Molecular Formula: C₆H₈O₇*C₃₁H₃₅FeNO₂
• Molecular Weight: 701.597
• Mol file: 1291080-42-6.mol

Synonyms:

Chemical Property of 1-[4-(3-dimethylammoniumpropoxy)phenyl]-1-(4-hydroxyphenyl)-2-ferrocenyl-but-1-ene citrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[4-(3-dimethylammoniumpropoxy)phenyl]-1-(4-hydroxyphenyl)-2-ferrocenyl-but-1-ene citrate

There total 1 articles about 1-[4-(3-dimethylammoniumpropoxy)phenyl]-1-(4-hydroxyphenyl)-2-ferrocenyl-but-1-ene citrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-[(4-(3-dimethylaminopropyloxy)phenyl)]-1’-(hydroxyphenyl)-2-ferrocenylbut-1-ene (287715-30-4,647010-84-2,646536-22-3) + citric acid (77-92-9,906507-37-7) → 1-[4-(3-dimethylammoniumpropoxy)phenyl]-1-(4-hydroxyphenyl)-2-ferrocenyl-but-1-ene citrate (1291080-42-6)

Guidance literature:

In tetrahydrofuran; diethyl ether; under Ar, Schlenk techniques; Fc compd. dissolved in THF, then Et2O added, then soln. of citric aicd in THF added dropwise, stirring (20 min); solid washed (Et2O), dried (vac.); traces of Et2O and THF;

DOI:10.1016/j.jorganchem.2010.09.015

upstream raw materials:

1-[(4-(3-dimethylaminopropyloxy)phenyl)]-1’-(hydroxyphenyl)-2-ferrocenylbut-1-ene

citric acid