N,N-Dibutyloctanamide

Base Information

• Chemical Name: N,N-Dibutyloctanamide
• CAS No.: 57303-23-8
• Molecular Formula: C16H33NO
• Molecular Weight: 255.444
• European Community (EC) Number: 260-670-7
• NSC Number: 24749
• DSSTox Substance ID: DTXSID30205925
• Nikkaji Number: J349.130G
• Wikidata: Q83079664
• Mol file: 57303-23-8.mol

Synonyms:N,N-Dibutyloctanamide;57303-23-8;Octanamide, N,N-dibutyl-;EINECS 260-670-7;AI3-31072;NSC24749;starbld0016299;Octanoic acid dibutylamide;SCHEMBL781384;DTXSID30205925;NSC 24749;NSC-24749;AKOS003865984

Chemical Property of N,N-Dibutyloctanamide

Chemical Property:

• Vapor Pressure: 0.00064mmHg at 25°C
• Refractive Index: 1.45
• Boiling Point: 309.4 °C at 760 mmHg
• Flash Point: 114.3 °C
• PSA: 20.31000
• Density: 0.86 g/cm³
• LogP: 4.77570
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 12
• Exact Mass: 255.256214676
• Heavy Atom Count: 18
• Complexity: 184

Purity/Quality:

99% ^*data from raw suppliers

N,N-DIBUTYLOCTANAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCC(=O)N(CCCC)CCCC

Technology Process of N,N-Dibutyloctanamide

There total 3 articles about N,N-Dibutyloctanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

Octanoic acid (124-07-2) + dibutylamine (111-92-2) → Ν,Ν-dibutyl-octanamide (57303-23-8)

Guidance literature:

at 160 ℃; for 65h; Dean-Stark;

Reference yield:

1-hexene (592-41-6,25067-06-5) + N,N-dibutylbromoacetamide (40124-27-4) → Ν,Ν-dibutyl-octanamide (57303-23-8)

Guidance literature:

With diborane; lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, room temp., 30 min, 2.) THF, -78 deg C, 30 min; room temp., 3 h;

DOI:10.1021/jo00074a046

Reference yield:

→ Ν,Ν-dibutyl-octanamide (57303-23-8)

Guidance literature:

upstream raw materials:

1-hexene

N,N-dibutylbromoacetamide

Octanoic acid

dibutylamine

Refernces

• 1、 -. "Water insoluble composition of an aldoxime extractant and an equilibrium modifier". . . Retrieved 2008/06/13.
• 2、 -. "Compositions comprising N,N-dialkylalkanamides". . . Retrieved 2008/06/13.