Technology Process of 2-Benzyl-1,2-dihydro-1,3-diphenyl-1,2,4-benzotriazin
There total 5 articles about 2-Benzyl-1,2-dihydro-1,3-diphenyl-1,2,4-benzotriazin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-phenylbenzo-1,2,4-triazine; phenyllithium;
In
tetrahydrofuran;
at -5 ℃;
benzyl bromide;
In
tetrahydrofuran;
DOI:10.1016/j.tet.2017.05.032
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 51 percent / HgO / ethanol / 1) reflux, 1 h, 2) room temp., 4 d
2: 1) H2, 2) BaO / 1) 5percent PdO/BaSO4 / 1) DMF, 2) room temp., 2 d
With
hydrogen; mercury(II) oxide; barium(II) oxide;
barium sulfate; trimethyleneglycol;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethylsulfoxide / 140 °C
2: 1) H2, 2) BaO / 1) 5percent PdO/BaSO4 / 1) DMF, 2) room temp., 2 d
With
hydrogen; barium(II) oxide;
barium sulfate; trimethyleneglycol;
In
dimethyl sulfoxide;
