Technology Process of C37H41N3O5
There total 5 articles about C37H41N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H32N2O5; phenylhydrazone of ethyl ester of glyoxalic acid;
With
potassium tert-butylate;
In
tetrahydrofuran;
at -78 ℃;
With
trifluoroacetic acid;
at -78 ℃;
for 2h;
DOI:10.1016/j.bmcl.2012.04.106
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 2,6-dimethylpyridine; HATU / tetrahydrofuran; N,N-dimethyl-formamide / 1 h / 20 °C
2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tri-n-octylsilane; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 70 °C
3.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C
4.1: dmap; acetic anhydride / tetrahydrofuran / 0.5 h / 20 °C
4.2: 16 h / 20 °C
5.1: potassium tert-butylate / tetrahydrofuran / -78 °C
5.2: 2 h / -78 °C
With
2,6-dimethylpyridine; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tri-n-octylsilane; potassium tert-butylate; acetic anhydride; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.106
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C
2.1: dmap; acetic anhydride / tetrahydrofuran / 0.5 h / 20 °C
2.2: 16 h / 20 °C
3.1: potassium tert-butylate / tetrahydrofuran / -78 °C
3.2: 2 h / -78 °C
With
dmap; potassium tert-butylate; acetic anhydride;
In
tetrahydrofuran;
DOI:10.1016/j.bmcl.2012.04.106
