3-(4-methoxyphenyl)-3-germatranylpropionic acid

Base Information

Chemical Name:3-(4-methoxyphenyl)-3-germatranylpropionic acid
CAS No.:214913-22-1
Molecular Formula:C₁₆H₂₃GeNO₆
Molecular Weight:397.952
Hs Code.:

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Chemical Property of 3-(4-methoxyphenyl)-3-germatranylpropionic acid

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Technology Process of 3-(4-methoxyphenyl)-3-germatranylpropionic acid

There total 1 articles about 3-(4-methoxyphenyl)-3-germatranylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-71-6,64114-46-1
triethanolamine

: 3-(4-methoxyphenyl)-3-germaniumsesquioxidepropionic acid

: 214913-22-1
3-(4-methoxyphenyl)-3-germatranylpropionic acid

Guidance literature:: In toluene; byproducts: H2O; under Ar, (HOCH2CH2)3N was added dropwise to toluene soln. of Ge-compd.,reflux for 6 h with constant removal of water; toluene was decanted, crystn. from 95 % hot EtOH, elem. anal.;
DOI:10.1081/SIM-100002047

Reference yield: 90.3%

: dibutyltin(IV) oxide

: 214913-22-1
3-(4-methoxyphenyl)-3-germatranylpropionic acid

: 214913-10-7
(CH₃(CH₂)3)2Sn(O₂CCH₂CH(C₆H₄OCH₃)Ge((OCH₂CH₂)3N))2(H₂O)

Guidance literature:: In toluene; refluxing Sn-compd. with 2 equiv. of Ge-compd. for 6 h; concn. (distn.), filtration, evapn. (vac.), recrystn. (CHCl3/petroleum ether); elem. anal.;
DOI:10.1016/S0022-328X(98)00607-X

Reference yield: 80.0%

: 214913-22-1
3-(4-methoxyphenyl)-3-germatranylpropionic acid

: 38047-49-3
bis((trimethylsilyl)methyl)tin dichloride

: 355018-21-2
bis(trimethylsilylmethyl)bis(3-(4-methoxyphenyl)-3-germatranyl)tin(IV) propionate

Guidance literature:: In ethanol; under Ar, Ge-compd. was added to mixt. of Sn-compd. and Et3N in EtOH, reflux for 6 h; soln. was cooled, EtOH was removed in vac., solid was extd. with CH2Cl2,elem. anal.;
DOI:10.1081/SIM-100002047