C₃₂H₂₇FN₂O₃

Base Information

Chemical Name:C₃₂H₂₇FN₂O₃
CAS No.:1373398-48-1
Molecular Formula:C₃₂H₂₇FN₂O₃
Molecular Weight:506.576
Hs Code.:

C<sub>32</sub>H<sub>27</sub>FN<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₃₂H₂₇FN₂O₃

Chemical Property:

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Technology Process of C₃₂H₂₇FN₂O₃

There total 6 articles about C₃₂H₂₇FN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₁₆BrFN₂

: 1373398-48-1
C₃₂H₂₇FN₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one; mineral oil / 3.08 h / 20 - 60 °C / Inert atmosphere

1.2: 3 h / 35 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 15 h / 50 °C

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydroxide / ethanol / 15 h / Reflux; Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydride; potassium carbonate; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; ethanol; N,N-dimethyl-formamide; mineral oil; 3.1: Suzuki coupling;
DOI:10.1248/cpb.60.164

Reference yield:

: 1373398-42-5
C₂₃H₁₈BrFN₂

: 1373398-48-1
C₃₂H₂₇FN₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydroxide / ethanol / 15 h / Reflux; Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 15 h / Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium carbonate; sodium hydroxide; In ethanol; N,N-dimethyl-formamide; 1: Suzuki coupling;
DOI:10.1248/cpb.60.164

Reference yield:

: 50709-33-6
2-bromophenylhydrazine hydrochloride

: 1373398-48-1
C₃₂H₂₇FN₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium acetate / ethanol / 20 h / Reflux

2.1: sodium hydride / 1-methyl-pyrrolidin-2-one; mineral oil / 3.08 h / 20 - 60 °C / Inert atmosphere

2.2: 3 h / 35 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide / 15 h / 50 °C

4.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium hydroxide / ethanol / 15 h / Reflux; Inert atmosphere

5.1: potassium carbonate / N,N-dimethyl-formamide / 15 h / Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium acetate; sodium hydride; potassium carbonate; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; ethanol; N,N-dimethyl-formamide; mineral oil; 4.1: Suzuki coupling;
DOI:10.1248/cpb.60.164