Technology Process of C55H80F3N5O16
There total 5 articles about C55H80F3N5O16 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
N,N-dimethyl acetamide; water;
at 20 ℃;
for 36.5h;
pH=6;
DOI:10.1016/j.tet.2003.12.053
- Guidance literature:
-
Multi-step reaction with 6 steps
1: n-Bu4NMnO4; pyridine / 1 h / 20 °C
2: 357 mg / 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide hydrochloride / dimethylformamide / 1 h / 20 °C
3: 94 percent / methanol / 0.12 h / 0 °C
4: 84 percent / Et3N / dimethylformamide / 0.5 h / 20 °C
5: trifluoroacetic acid / CH2Cl2 / 0.5 h / 0 °C
6: 6.8 mg / NaOH / N,N-dimethyl-acetamide; H2O / 36.5 h / 20 °C / pH 6
With
pyridine; sodium hydroxide; tetra-n-butylammonium permanganate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.12.053
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 357 mg / 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide hydrochloride / dimethylformamide / 1 h / 20 °C
2: 94 percent / methanol / 0.12 h / 0 °C
3: 84 percent / Et3N / dimethylformamide / 0.5 h / 20 °C
4: trifluoroacetic acid / CH2Cl2 / 0.5 h / 0 °C
5: 6.8 mg / NaOH / N,N-dimethyl-acetamide; H2O / 36.5 h / 20 °C / pH 6
With
sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.12.053
