Technology Process of C16H12Cl2O4
There total 1 articles about C16H12Cl2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
aluminum (III) chloride;
In
dichloromethane;
at 5 - 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1039/c3nj00032j
- Guidance literature:
-
With
hydroxylamine hydrochloride;
In
ethanol;
for 5h;
Reflux;
Inert atmosphere;
DOI:10.1039/c3nj00032j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride / ethanol / 5 h / Reflux; Inert atmosphere
2: sodium tetrahydroborate; iodine / tetrahydrofuran / 7.5 h / 0 °C / Reflux; Inert atmosphere
3: triethylamine / tetrahydrofuran / 2 h / 5 - 20 °C / Inert atmosphere
4: thionyl chloride / toluene / 3 h / 80 °C / Inert atmosphere
5: sodium hydroxide / methanol / 1 h / 50 °C / Inert atmosphere
With
sodium tetrahydroborate; thionyl chloride; hydroxylamine hydrochloride; iodine; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; toluene;
DOI:10.1039/c3nj00032j