Technology Process of C28H31NO4
There total 3 articles about C28H31NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
caffeic acid;
With
2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide;
In
1,4-dioxane;
at 20 ℃;
3-O-methyl-17β-aminoestra-1,3,5(10),6-tetraene-3-ol;
In
1,4-dioxane;
for 0.0666667h;
Microwave irradiation;
Inert atmosphere;
DOI:10.3184/174751912X13419346932954
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: aluminium; mercury dichloride; ethanol / water / 24 h / Reflux
2.1: 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide / 1,4-dioxane / 20 °C
2.2: 0.07 h / Microwave irradiation; Inert atmosphere
With
ethanol; 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide; aluminium; mercury dichloride;
In
1,4-dioxane; water;
DOI:10.3184/174751912X13419346932954
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydroxylamine hydrochloride / ethanol; water / 11.5 h / 50 °C
2.1: aluminium; mercury dichloride; ethanol / water / 24 h / Reflux
3.1: 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide / 1,4-dioxane / 20 °C
3.2: 0.07 h / Microwave irradiation; Inert atmosphere
With
ethanol; 2,3,4,5,6-pentafluorophenol; hydroxylamine hydrochloride; dicyclohexyl-carbodiimide; aluminium; mercury dichloride;
In
1,4-dioxane; ethanol; water;
DOI:10.3184/174751912X13419346932954
