C₃₁H₄₄N₂O₆Si

Base Information

Chemical Name:C₃₁H₄₄N₂O₆Si
CAS No.:1567326-30-0
Molecular Formula:C₃₁H₄₄N₂O₆Si
Molecular Weight:568.786
Hs Code.:

C<sub>31</sub>H<sub>44</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₃₁H₄₄N₂O₆Si

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Technology Process of C₃₁H₄₄N₂O₆Si

There total 11 articles about C₃₁H₄₄N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 530-26-7
D-Mannose

: 1567326-30-0
C₃₁H₄₄N₂O₆Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: iodine / 16 h / 20 °C

2.1: sodium cyanide / water / 12 h / 50 °C

2.2: 12 h / 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

3.2: 20 h / 20 °C

4.1: acetic acid / water / 3.5 h / 50 °C

5.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

7.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

8.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

9.1: tetrahydrofuran; methanol / 2 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide

11.1: N-ethyl-N,N-diisopropylamine / dichloromethane

With pyridine; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; iodine; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4
2,3:5,6-di-O-isopropylidene-D-mannofuranose

: 1567326-30-0
C₃₁H₄₄N₂O₆Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium cyanide / water / 12 h / 50 °C

1.2: 12 h / 20 °C

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

2.2: 20 h / 20 °C

3.1: acetic acid / water / 3.5 h / 50 °C

4.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

6.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

7.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

8.1: tetrahydrofuran; methanol / 2 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane

With pyridine; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 137126-24-0
(3aR,4R,7S,7aR)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-7-hydroxy-2,2-dimethyltetrahydro-[1,3]-dioxolo-[4,5-c]-pyran-6-one

: 1567326-30-0
C₃₁H₄₄N₂O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

1.2: 20 h / 20 °C

2.1: acetic acid / water / 3.5 h / 50 °C

3.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

5.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

6.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

7.1: tetrahydrofuran; methanol / 2 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane

With pyridine; dmap; trifluoromethylsulfonic anhydride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;