N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid

Base Information

• Chemical Name: N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid
• CAS No.: 1586819-23-9
• Molecular Formula: C₂₈H₂₄Cl₆N₂O₄
• Molecular Weight: 665.228

Synonyms:

Chemical Property of N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid

Chemical Property:

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Technology Process of N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid

There total 1 articles about N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.05,10]undec-2-ene-7,8-dicarboxylic acid anhydride (42224-21-5) + 4,4'-methylene-bis[3-methoxy]benzenamine → N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.05,10]undec-2-ene-7,8-dicarboxylic acid (1586819-23-9)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 6h;

DOI:10.1134/S1070428014020122

Reference yield: 88.0%

maleic anhydride (108-31-6) + N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.05,10]undec-2-ene-7,8-dicarboxylic acid (1586819-23-9) → N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.05,10]undec-2-ene-7,8-dicarboxylic acid (1586819-33-1)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 6h;

DOI:10.1134/S1070428014020122

Reference yield:

N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.05,10]undec-2-ene-7,8-dicarboxylic acid (1586819-23-9) → N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid (1586819-49-9)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 6 h / 150 °C

2: pyridine / N,N-dimethyl-formamide / 20 °C

With pyridine; In N,N-dimethyl-formamide;

DOI:10.1134/S1070428014020122

upstream raw materials:

endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid anhydride

Downstream raw materials:

N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid

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