Technology Process of C19H23(2)H2N3OSi
There total 6 articles about C19H23(2)H2N3OSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 2.7 g / 40percent NaOD / D2O / 3 h / Heating
2: 2.1 g / HCl / 4 h / Heating
3: 1.0 g / PCl3 / CHCl3 / 1 h / Heating
4: 0.7 g / hydrazine hydrate / 0.5 h / Heating
5: ethanol / 0.5 h
6: dimethylformamide
With
hydrogenchloride; deuteriated sodium hydroxide; hydrazine hydrate; phosphorus trichloride;
In
ethanol; chloroform; water-d2; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1637
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 2.1 g / HCl / 4 h / Heating
2: 1.0 g / PCl3 / CHCl3 / 1 h / Heating
3: 0.7 g / hydrazine hydrate / 0.5 h / Heating
4: ethanol / 0.5 h
5: dimethylformamide
With
hydrogenchloride; hydrazine hydrate; phosphorus trichloride;
In
ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1637
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 0.7 g / hydrazine hydrate / 0.5 h / Heating
2: ethanol / 0.5 h
3: dimethylformamide
With
hydrazine hydrate;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.1637