2'-Aminohexestrol Dimethyl Ether

Base Information

Chemical Name:2'-Aminohexestrol Dimethyl Ether
CAS No.:77153-69-6
Molecular Formula:C₂₀H₂₇NO₂
Molecular Weight:313.44
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Aminohexestrol Dimethyl Ether

Chemical Property:

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Technology Process of 2'-Aminohexestrol Dimethyl Ether

There total 1 articles about 2'-Aminohexestrol Dimethyl Ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130-78-9
meso-3,4-Bis(4-methoxyphenyl)hexan

: 77153-69-6
2'-Aminohexestrol Dimethyl Ether

Guidance literature:: With bromine; potassium amide; Yield given. Multistep reaction; 1.) CCl₄, from 0 deg C to 5 deg C, 30 min, 2.) ammonia (liquid), THF, 1.5 h;
DOI:10.1021/jo00325a017

Reference yield:

: 77153-69-6
2'-Aminohexestrol Dimethyl Ether

: 77153-71-0
2'-Fluorohexestrol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) concentrated HCl, NaNO₂ / 1.) 1:1 CH₃COCH₃-H₂O, 0 deg C, 30 min, 2.) 30 min

2: 41 percent / 48percent aqueous HF / 1.) room temperature, 30 min, 2.) 50 deg C, 10 min

3: 83 percent / BBr₃ / CHCl₃ / 0.33 h / Heating

With hydrogenchloride; hydrogen fluoride; boron tribromide; sodium nitrite; In chloroform;
DOI:10.1021/jo00325a017

Reference yield:

: 77153-69-6
2'-Aminohexestrol Dimethyl Ether

: 5025-38-7
9,10-Diethyl-3,6-dimethoxy-phenanthren

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) concentrated HCl, NaNO₂ / 1.) 1:1 CH₃COCH₃-H₂O, 0 deg C, 30 min, 2.) 30 min

2: 50 percent / 48percent aqueous HF / 1.) room temperature, 30 min, 2.) 50 deg C, 10 min

3: 54 percent / Dichlorodicyanoquinone (DDQ) / benzene

With hydrogenchloride; hydrogen fluoride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium nitrite; In benzene;
DOI:10.1021/jo00325a017