2'-Fluorohexestrol

Base Information

Chemical Name:2'-Fluorohexestrol
CAS No.:77153-71-0
Molecular Formula:C₁₈H₂₁FO₂
Molecular Weight:288.362
Hs Code.:

Synonyms:2'-Fluorohexestrol

Suppliers and Price of 2'-Fluorohexestrol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Fluorohexestrol

Chemical Property:

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Technology Process of 2'-Fluorohexestrol

There total 4 articles about 2'-Fluorohexestrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 77153-70-9
2'-Fluorohexestrol Dimethyl Ether

: 77153-71-0
2'-Fluorohexestrol

Guidance literature:: With boron tribromide; In chloroform; for 0.333333h; Heating;
DOI:10.1021/jo00325a017

Reference yield:

: 130-78-9
meso-3,4-Bis(4-methoxyphenyl)hexan

: 77153-71-0
2'-Fluorohexestrol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Br₂, 2.) KNH₂ / 1.) CCl₄, from 0 deg C to 5 deg C, 30 min, 2.) ammonia (liquid), THF, 1.5 h

2: 1.) concentrated HCl, NaNO₂ / 1.) 1:1 CH₃COCH₃-H₂O, 0 deg C, 30 min, 2.) 30 min

3: 41 percent / 48percent aqueous HF / 1.) room temperature, 30 min, 2.) 50 deg C, 10 min

4: 83 percent / BBr₃ / CHCl₃ / 0.33 h / Heating

With hydrogenchloride; hydrogen fluoride; bromine; boron tribromide; potassium amide; sodium nitrite; In chloroform;
DOI:10.1021/jo00325a017

Reference yield:

: 77153-69-6
2'-Aminohexestrol Dimethyl Ether

: 77153-71-0
2'-Fluorohexestrol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) concentrated HCl, NaNO₂ / 1.) 1:1 CH₃COCH₃-H₂O, 0 deg C, 30 min, 2.) 30 min

2: 41 percent / 48percent aqueous HF / 1.) room temperature, 30 min, 2.) 50 deg C, 10 min

3: 83 percent / BBr₃ / CHCl₃ / 0.33 h / Heating

With hydrogenchloride; hydrogen fluoride; boron tribromide; sodium nitrite; In chloroform;
DOI:10.1021/jo00325a017