Technology Process of C26H16(2)H5NO2SSe
There total 6 articles about C26H16(2)H5NO2SSe which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B
2: toluene / 6 h / Heating; thermal or base catalysed rearrangement
In
toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 86.1 percent / dimethylformamide / 4 h / 120 °C
2: 99.6 percent / diethyl ether / 1 h / Heating
3: 69.2 percent / 80percent H2SO4 / 0.5 h / 95 °C
4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B
5: toluene / 6 h / Heating; thermal or base catalysed rearrangement
With
sulfuric acid;
In
diethyl ether; N,N-dimethyl-formamide; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 86.1 percent / dimethylformamide / 4 h / 120 °C
2: 99.6 percent / diethyl ether / 1 h / Heating
3: 69.2 percent / 80percent H2SO4 / 0.5 h / 95 °C
4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B
5: toluene / 6 h / Heating; thermal or base catalysed rearrangement
With
sulfuric acid;
In
diethyl ether; N,N-dimethyl-formamide; toluene; acetonitrile;