rel-(8aS)-6-methoxycarbonyl-1,2,3,7,8,8a-hexahydrobenz--indolizine

Base Information

• Chemical Name: rel-(8aS)-6-methoxycarbonyl-1,2,3,7,8,8a-hexahydrobenz-
• Molecular Formula: C₁₄H₁₅NO₂
• Molecular Weight: 229.279

Synonyms:

Chemical Property of rel-(8aS)-6-methoxycarbonyl-1,2,3,7,8,8a-hexahydrobenz-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

There total 2 articles about rel-(8aS)-6-methoxycarbonyl-1,2,3,7,8,8a-hexahydrobenz--indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

1-(2-bromobenzyl)-1,4-dihydro-3-methoxycarbonylpyridine (126225-70-5) → methyl 1-benzyl-1,4-dihydropyridine-3-carboxylate (57355-62-1) + rel-(8aS)-6-methoxycarbonyl-1,2,3,7,8,8a-hexahydrobenz--indolizine (126225-84-1) + rel-(8S,8aS)-8-methoxycarbonylperhydrobenzindolizine (126225-76-1,126225-77-2)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 3h; Heating;

DOI:10.1016/S0040-4020(01)81101-7

Reference yield: 22.0%

1-(2-bromobenzyl)-1,4-dihydro-3-methoxycarbonylpyridine (126225-70-5) → methyl 1-benzyl-1,4-dihydropyridine-3-carboxylate (57355-62-1) + rel-(8aS)-6-methoxycarbonyl-1,2,3,7,8,8a-hexahydrobenz--indolizine (126225-84-1)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 1.5h; Heating;

DOI:10.1016/S0040-4020(01)81101-7

upstream raw materials:

1-(2-bromobenzyl)-1,4-dihydro-3-methoxycarbonylpyridine

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