Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester

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Chemical Name:Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester
CAS No.:199597-32-5
Molecular Formula:C₄₀H₄₀ClN₄O₈PS₂
Molecular Weight:835.338
Hs Code.:

Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester

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Chemical Property of Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester

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Technology Process of Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester

There total 3 articles about Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98796-51-1
5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-[O-(2-cyanoethyl)-N,N'-diisopropylphosphoramidite]

: 199597-32-5
Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂S, tetrazole

2: S₈, lutidine / toluene

3: NaI

With 1H-tetrazole; sulfur; lutidine; hydrogen sulfide; sodium iodide; In toluene;
DOI:10.1080/07328319708006243

Reference yield:

: 199597-29-0
C₃₄H₃₆N₃O₈PS

: 199597-32-5
Dithiophosphoric acid O-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl] ester S-(4-chloro-pyridin-2-ylmethyl) ester O'-(2-cyano-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: S₈, lutidine / toluene

2: NaI

With sulfur; lutidine; sodium iodide; In toluene;
DOI:10.1080/07328319708006243