glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

Base Information

Chemical Name:glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate
CAS No.:110582-53-1
Molecular Formula:C₁₆H₂₆N₃O₅P
Molecular Weight:371.373
Hs Code.:

<N-<N-<(phenylmethoxy)carbonyl>glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

Synonyms:

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Chemical Property of glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

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Technology Process of glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

There total 4 articles about glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 110582-51-9,110582-52-0
1-amino-3-methylbutyl(methoxy)phosphonamidate

: 110582-53-1,110582-54-2
glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

Guidance literature:: With diphenyl-phosphinic acid; triethylamine; In tetrahydrofuran; 0 deg C to 21 deg C;

Reference yield:

: 90763-54-5
methyl <1--3-methylbutyl>phosphonate

: 110582-53-1,110582-54-2
glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

Guidance literature:: Multi-step reaction with 4 steps

1: 19 percent / DDPA, triethylamine / CH₂Cl₂ / 18 h / 21 °C

2: 74 percent / ammonia gas / CH₂Cl₂ / 0.17 h / 21 °C

3: 95 percent / H₂ / 10percent Pd/C / methanol / 1 h

4: 50 percent / DPPA, triethylamine / tetrahydrofuran / 0 deg C to 21 deg C

With diphenyl-phosphinic acid; ammonia; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 110582-37-1,110582-38-2
phenylmethyl <1--3-methylbutyl>carbamate

: 110582-53-1,110582-54-2
glycyl>-1-amino-3-methylbutyl>(methoxy)phosphonamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / 10percent Pd/C / methanol / 1 h

2: 50 percent / DPPA, triethylamine / tetrahydrofuran / 0 deg C to 21 deg C

With diphenyl-phosphinic acid; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;