carbonyldiiodo-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(III)

Base Information

• Chemical Name: carbonyldiiodo-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(III)
• CAS No.: 331821-79-5
• Molecular Formula: C₁₈H₂₂CoI₂NO
• Molecular Weight: 581.181
• Mol file: 331821-79-5.mol

Synonyms:

Chemical Property of carbonyldiiodo-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(III)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of carbonyldiiodo-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(III)

There total 1 articles about carbonyldiiodo-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

dicarbonyl-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(I) (331821-76-2) + iodine (7553-56-2,12190-71-5,8031-47-8) → carbonyldiiodo-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(III) (331821-79-5)

Guidance literature:

In diethyl ether; under N2 atm. soln. I2 in Et2O was added dropwise at -30°C to soln. complex in Et2O and stirred at room temp. for 16 h; react. mixt. was concd., crystals were washed with hexane and dried in vac.;

DOI:10.1021/om0007163

upstream raw materials:

dicarbonyl-eta.5-(1-(2-N,N-dimethylaminophenyl)-2,3,4,5-tetramethylcyclopentadienyl)cobalt(I)

iodine