(3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester

Base Information

• Chemical Name: (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester
• CAS No.: 92693-20-4
• Molecular Formula: C₃₄H₅₆N₄O₉
• Molecular Weight: 664.84

Synonyms:

Chemical Property of (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester

There total 1 articles about (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-D-pheO-succinyl (3674-18-8) + H-Sta-Ala-Sta-OCH3 trifluoroacetate (102281-31-2) → (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester (92693-20-4)

Guidance literature:

With N-ethylmorpholine;; benzotriazol-1-ol; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

DOI:10.1021/jm00157a006

Reference yield:

(3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester (92693-20-4) + trifluoroacetic acid (76-05-1) → (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid (92608-75-8,92693-22-6)

Guidance literature:

In dichloromethane; for 0.5h;

DOI:10.1021/jm00157a006

upstream raw materials:

Boc-D-pheO-succinyl

H-Sta-Ala-Sta-OCH₃ trifluoroacetate

Downstream raw materials:

(3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid

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