(3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid

Base Information

• Chemical Name: (3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid
• CAS No.: 92608-75-8
• Molecular Formula: C₂HF₃O₂*C₂₉H₄₈N₄O₇
• Molecular Weight: 678.747

Synonyms:

Chemical Property of (3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid

Chemical Property:

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Safty Information:

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Useful:

Technology Process of (3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid

There total 3 articles about (3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-D-pheO-succinyl (3674-18-8) → (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid (92608-75-8,92693-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: N-ethylmorpholine (NEM), 1-hydroxybenzotriazol (HOBT) / dimethylformamide / 48 h / Ambient temperature

2: CH₂Cl₂ / 0.5 h

With N-ethylmorpholine;; benzotriazol-1-ol; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm00157a006

Reference yield:

(3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester (92693-20-4) + trifluoroacetic acid (76-05-1) → (3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid (92608-75-8,92693-22-6)

Guidance literature:

In dichloromethane; for 0.5h;

DOI:10.1021/jm00157a006

Reference yield:

(3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester (92608-73-6) + trifluoroacetic acid (76-05-1) → (3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-Amino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester; compound with trifluoro-acetic acid (92608-75-8,92693-22-6)

Guidance literature:

In dichloromethane; for 0.5h;

DOI:10.1021/jm00157a006

upstream raw materials:

(3S,4S)-4-{(S)-2-[(3S,4S)-4-((R)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester

trifluoroacetic acid

Boc-D-pheO-succinyl

(3S,4S)-4-{(S)-2-[(3S,4S)-4-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-3-hydroxy-6-methyl-heptanoylamino]-propionylamino}-3-hydroxy-6-methyl-heptanoic acid methyl ester

Downstream raw materials:

Z-Phe-D-Phe-Sta-Ala-Sta-OCH₃

Boc-D-Phe-Phe-Sta-Ala-Sta-OCH₃

Iva-Phe-Phe-Sta-Ala-Sta-OCH₃

t-BuCH₂CO-Phe-Phe-Sta-Ala-Sta-OCH₃

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