Perfluorohexylphosphonic Acid 4-MethylbenzaMine

Base Information

• Chemical Name: Perfluorohexylphosphonic Acid 4-MethylbenzaMine
• CAS No.: 1263361-02-9
• Molecular Formula: C₆H₂F₁₃O₃P*C₇H₉N
• Molecular Weight: 507.188
• Mol file: 1263361-02-9.mol

Synonyms:

Chemical Property of Perfluorohexylphosphonic Acid 4-MethylbenzaMine

Chemical Property:

Purity/Quality:

PerfluorohexylphosphonicAcid4-Methylbenzamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Perfluorohexylphosphonic Acid 4-Methylbenzamine has shown to be useful in the areas of antifoaming agents, HPLC and even fluorinated ion-exchange membranes for fuel energy and cells.

Technology Process of Perfluorohexylphosphonic Acid 4-MethylbenzaMine

There total 3 articles about Perfluorohexylphosphonic Acid 4-MethylbenzaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-perfluorohexyl iodide (355-43-1) → C6H2F13O3P*C7H9N (1263361-02-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: ethylmagnesium bromide / diethyl ether / 1 h / -78 °C / Inert atmosphere

1.2: 6 h / -78 °C / Inert atmosphere

2.1: water / diethyl ether / 0 °C / Inert atmosphere

3.1: dihydrogen peroxide / diethyl ether / Inert atmosphere

4.1: diethyl ether / Inert atmosphere

With ethylmagnesium bromide; water; dihydrogen peroxide; In diethyl ether;

DOI:10.1021/ic102063e

Reference yield:

C6H2F13O2P (1263360-98-0) → C6H2F13O3P*C7H9N (1263361-02-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dihydrogen peroxide / diethyl ether / Inert atmosphere

2: diethyl ether / Inert atmosphere

With dihydrogen peroxide; In diethyl ether;

DOI:10.1021/ic102063e

Reference yield:

Perfluorhexylphosphonsaeure (40143-76-8) + p-toluidine (106-49-0,12221-03-3) → C6H2F13O3P*C7H9N (1263361-02-9)

Guidance literature:

In diethyl ether; Inert atmosphere;

DOI:10.1021/ic102063e

upstream raw materials:

Perfluorhexylphosphonsaeure

p-toluidine

C₆H₂F₁₃O₂P

n-perfluorohexyl iodide

Refernces