C₄₆H₈₆O₁₀SSi₃

Base Information

Chemical Name:C₄₆H₈₆O₁₀SSi₃
CAS No.:1431725-94-8
Molecular Formula:C₄₆H₈₆O₁₀SSi₃
Molecular Weight:915.505
Hs Code.:

C<sub>46</sub>H<sub>86</sub>O<sub>10</sub>SSi<sub>3</sub>

Synonyms:

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Chemical Property of C₄₆H₈₆O₁₀SSi₃

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Technology Process of C₄₆H₈₆O₁₀SSi₃

There total 13 articles about C₄₆H₈₆O₁₀SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431725-93-7
C₄₆H₈₈O₁₀SSi₃

: 1431725-94-8
C₄₆H₈₆O₁₀SSi₃

Guidance literature:: With dipyridine chromium trioxide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.201203406

Reference yield:

: 1431725-64-2
C₃₈H₆₈O₄Si₃

: 1431725-94-8
C₄₆H₈₆O₁₀SSi₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride; pyridine / dichloromethane / 0.05 h / 0 °C

2.1: H₃N*FH*3H₂O / methanol / 12 h / Inert atmosphere; Reflux

3.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - 0 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

5.1: dipyridine chromium trioxide / dichloromethane / 0 - 20 °C

With pyridine; n-butyllithium; thionyl chloride; H₃N*FH*3H₂O; dipyridine chromium trioxide; Dess-Martin periodane; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1002/anie.201203406

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1431725-94-8
C₄₆H₈₆O₁₀SSi₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere

2.1: thionyl chloride; pyridine / dichloromethane / 0.05 h / 0 °C

3.1: H₃N*FH*3H₂O / methanol / 12 h / Inert atmosphere; Reflux

4.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 - 0 °C / Inert atmosphere

5.2: 1 h / -78 °C / Inert atmosphere

6.1: dipyridine chromium trioxide / dichloromethane / 0 - 20 °C

With pyridine; 1H-imidazole; n-butyllithium; thionyl chloride; H₃N*FH*3H₂O; dipyridine chromium trioxide; Dess-Martin periodane; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201203406