<9-Brommethyl-fluoren-9-yl>--sulfon

Base Information

• Chemical Name: <9-Brommethyl-fluoren-9-yl>--sulfon
• CAS No.: 95703-46-1
• Molecular Formula: C₂₁H₁₇BrO₂S
• Molecular Weight: 413.335

Synonyms:

Chemical Property of <9-Brommethyl-fluoren-9-yl>--sulfon

Chemical Property:

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Technology Process of <9-Brommethyl-fluoren-9-yl>--sulfon

There total 1 articles about <9-Brommethyl-fluoren-9-yl>--sulfon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-tolyl 9-fluorenyl sulfone (102001-66-1) + 1,1-dibromomethane (74-95-3) → <9-Brommethyl-fluoren-9-yl>--sulfon (95703-46-1)

Guidance literature:

With sodium methylate; In methanol; N,N-dimethyl-formamide;

DOI:10.1139/v64-215

Reference yield:

<9-Brommethyl-fluoren-9-yl>--sulfon (95703-46-1) → (9-Hydroxymethyl-fluoren-9-yl)-(p-tolyl)-sulfon (94866-91-8)

Guidance literature:

Multistep reaction; (i) CF₃CO₂Ag, CF₃CO₂H, (ii) aq. HCO₂H;

DOI:10.1139/v64-215

upstream raw materials:

p-tolyl 9-fluorenyl sulfone

1,1-dibromomethane

Downstream raw materials:

(9-Hydroxymethyl-fluoren-9-yl)-(p-tolyl)-sulfon

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