O²,O³-diacetyl-O⁴-trityl-D-erythrose-diethyldithioacetal

Base Information

• Chemical Name: O²,O³-diacetyl-O⁴-trityl-D-erythrose-diethyldithioacetal
• CAS No.: 119927-08-1
• Molecular Formula: C₃₁H₃₆O₅S₂
• Molecular Weight: 552.756

Synonyms:

Chemical Property of O²,O³-diacetyl-O⁴-trityl-D-erythrose-diethyldithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of O²,O³-diacetyl-O⁴-trityl-D-erythrose-diethyldithioacetal

There total 1 articles about O²,O³-diacetyl-O⁴-trityl-D-erythrose-diethyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-erythrose (583-50-6) + ethanethiol (75-08-1) → O2,O3-diacetyl-O4-trityl-D-erythrose-diethyldithioacetal (119927-08-1)

Guidance literature:

With hydrogenchloride; methanol; Behandeln des Reaktionsprodukts in Pyridin mit Tritylchlorid und anschliessend mit Acetanhydrid;

DOI:10.1021/ja01627a053

Reference yield:

O2,O3-diacetyl-O4-trityl-D-erythrose-diethyldithioacetal (119927-08-1) → L-O1-trityl-erythritol (102657-29-4)

Guidance literature:

With barium methoxide; mercury dichloride; mercury(II) oxide; anschliessend Behandeln mit NaBH₄;

DOI:10.1021/ja01596a046

Reference yield:

O2,O3-diacetyl-O4-trityl-D-erythrose-diethyldithioacetal (119927-08-1) → D-O1,O2,O3-tribenzoyl-O4-trityl-erythritol (50622-05-4)

Guidance literature:

Multi-step reaction with 2 steps

1: barium methylate; HgO; HgCl₂ / anschliessend Behandeln mit NaBH₄

With barium methoxide; mercury dichloride; mercury(II) oxide;

DOI:10.1021/ja01596a046

upstream raw materials:

D-erythrose

ethanethiol

Downstream raw materials:

L-O¹-trityl-erythritol

D-O¹,O²,O³-tribenzoyl-O⁴-trityl-erythritol

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