Technology Process of 4-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)vinyl)benzaldehyde oxime
There total 2 articles about 4-(1-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)vinyl)benzaldehyde oxime which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / 20 °C
1.2: 1 h / 0 °C / Cooling with ice
2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C
3.1: hydroxylamine hydrochloride / methanol / 20 °C
With
hydroxylamine hydrochloride; chloroformic acid ethyl ester; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; methanol; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C
2: hydroxylamine hydrochloride / methanol / 20 °C
With
hydroxylamine hydrochloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
methanol; dimethyl sulfoxide;
