Z-D-Ala-D-HyIv-L-Val-L-HyIv-D-Ala-D-HyIv-L-Val-L-HyIv

Base Information

• Chemical Name: Z-D-Ala-D-HyIv-L-Val-L-HyIv-D-Ala-D-HyIv-L-Val-L-HyIv
• CAS No.: 31508-93-7
• Molecular Formula: C₄₄H₆₈N₄O₁₅
• Molecular Weight: 893.042
• Mol file: 31508-93-7.mol

Synonyms:

Chemical Property of Z-D-Ala-D-HyIv-L-Val-L-HyIv-D-Ala-D-HyIv-L-Val-L-HyIv

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Z-D-Ala-D-HyIv-L-Val-L-HyIv-D-Ala-D-HyIv-L-Val-L-HyIv

There total 24 articles about Z-D-Ala-D-HyIv-L-Val-L-HyIv-D-Ala-D-HyIv-L-Val-L-HyIv which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Z-L-Ala-L-HyIv (31508-83-5,31508-84-6,31509-05-4) → Z-L-Ala-L-HyIv-D-Val-D-HyIv-L-Ala-L-HyIv-D-Val-D-HyIv (31508-93-7,31508-94-8,31509-10-1)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) SOCl₂, (ii) /BRN= 2417866/, Et₃N, benzene

2: H₂ / Pd / methanol

3: (i) SOCl₂, (ii) /BRN= 2633973/, Et₃N, benzene

4: CF₃CO₂H

With hydrogen; trifluoroacetic acid; palladium; In methanol;

DOI:10.1007/BF00565352

Reference yield:

Z-D-Ala-L-HyIv-OH (31508-83-5,31508-84-6,31509-05-4) → Z-D-Ala-L-HyIv-L-Val-D-HyIv-D-Ala-L-HyIv-L-Val-D-HyIv (31508-93-7,31508-94-8,31509-10-1)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) SOCl₂, (ii) /BRN= 2417867/, Et₃N, benzene

2: H₂ / Pd / methanol

3: (i) SOCl₂, (ii) /BRN= 2633974/, Et₃N, benzene

4: CF₃CO₂H

With hydrogen; trifluoroacetic acid; palladium; In methanol;

DOI:10.1007/BF00565352

Reference yield:

Z-D-Ala-D-HyIv-OtBu (31508-82-4) → Z-D-Ala-D-HyIv-L-Val-L-HyIv-D-Ala-D-HyIv-L-Val-L-HyIv (31508-93-7,31508-94-8,31509-10-1)

Guidance literature:

Multi-step reaction with 5 steps

1: TsOH / benzene

2: (i) SOCl₂, (ii) /BRN= 6132054/, Et₃N, benzene

3: H₂ / Pd / methanol

4: (i) SOCl₂, (ii) /BRN= 2633975/, Et₃N, benzene

5: CF₃CO₂H

With hydrogen; toluene-4-sulfonic acid; trifluoroacetic acid; palladium; In methanol; benzene;

DOI:10.1007/BF00565352

upstream raw materials:

Z-L-Ala-L-HyIv-D-Val-D-HyIv-L-Ala-L-HyIv-D-Val-D-HyIv-OtBu

N-Cbz-Ala

Z-L-Ala-L-HyIv

Z-L-Ala-L-HyIv-OtBu