C₁₂H₁₃BrFN₃O₂

Base Information

Chemical Name:C₁₂H₁₃BrFN₃O₂
CAS No.:1202578-70-8
Molecular Formula:C₁₂H₁₃BrFN₃O₂
Molecular Weight:330.157
Hs Code.:

C<sub>12</sub>H<sub>13</sub>BrFN<sub>3</sub>O<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₃BrFN₃O₂

Chemical Property:

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Technology Process of C₁₂H₁₃BrFN₃O₂

There total 6 articles about C₁₂H₁₃BrFN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1202578-67-3
C₁₂H₁₁BrFN₃O₄

: 1202578-70-8
C₁₂H₁₃BrFN₃O₂

Guidance literature:: With iron; ammonium chloride; In ethanol; water; Reflux;
DOI:10.1021/jf9026298

Reference yield:

: 1202578-62-8
C₁₁H₁₄BrFN₂O

: 1202578-70-8
C₁₂H₁₃BrFN₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / toluene / 20 °C / Inert atmosphere; Reflux

2: sulfuric acid; nitric acid / Cooling with ice

3: iron; ammonium chloride / ethanol; water / Reflux

With sulfuric acid; nitric acid; iron; ammonium chloride; triethylamine; In ethanol; water; toluene;
DOI:10.1021/jf9026298

Reference yield:

: 571170-91-7
(2-bromo-4-fluorophenyl)hydrazine hydrochloride

: 1202578-70-8
C₁₂H₁₃BrFN₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / dichloromethane; water / 0.5 h / Cooling with ice

2: dichloromethane / 20 °C

3: triethylamine / toluene / 20 °C / Inert atmosphere; Reflux

4: sulfuric acid; nitric acid / Cooling with ice

5: iron; ammonium chloride / ethanol; water / Reflux

With sulfuric acid; nitric acid; iron; ammonium chloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; toluene;
DOI:10.1021/jf9026298