11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate

Base Information

Chemical Name:11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate
CAS No.:78019-08-6
Molecular Formula:BF₄*C₂₉H₂₆N
Molecular Weight:475.337
Hs Code.:

11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzo<h>quinolinium Tetrafluoroborate

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Chemical Property of 11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate

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Technology Process of 11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate

There total 5 articles about 11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5,6-Dihydro-7-phenylcyclopenteno<1,2-b>benzochromenylium Tetrafluoroborate

: 100-46-9
benzylamine

: 78019-08-6
11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate

Guidance literature:: In ethanol; superdry EtOH (Mg);
DOI:10.1021/jo00332a013

Reference yield:

: 6261-32-1
2-benzylidene-1-tetralone

: 78019-08-6
11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Molecular sieves, 2.) AcOH / 1.) toluene, reflux, 12 h, 2.) EtOH, H₂O, 20 deg C, 72 h

2: 76 percent / Benzylideneacetophenone, BF₃*Et₂O / 2 h / 100 °C

3: 95 percent / ethanol / superdry EtOH (Mg)

With molecular sieve; boron trifluoride diethyl etherate; acetic acid; benzalacetophenone; In ethanol;
DOI:10.1021/jo00332a013

Reference yield:

: 1614-92-2
1-(N-piperidino)cyclopentene

: 78019-08-6
11-Benzyl-5,6-dihydro-7-phenylcyclopenteno<1,2-b>benzoquinolinium Tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Molecular sieves, 2.) AcOH / 1.) toluene, reflux, 12 h, 2.) EtOH, H₂O, 20 deg C, 72 h

2: 76 percent / Benzylideneacetophenone, BF₃*Et₂O / 2 h / 100 °C

3: 95 percent / ethanol / superdry EtOH (Mg)

With molecular sieve; boron trifluoride diethyl etherate; acetic acid; benzalacetophenone; In ethanol;
DOI:10.1021/jo00332a013