2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene

Base Information

Chemical Name:2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene
CAS No.:1544740-35-3
Molecular Formula:C₁₃H₁₉BrO₂S
Molecular Weight:319.263
Hs Code.:

Synonyms:

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Chemical Property of 2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene

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Technology Process of 2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene

There total 9 articles about 2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1544740-28-4
ethyl 3-(4-bromo-3,5-dimethylphenyl)propanoate

: 1544740-35-3
2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene

Guidance literature:: Multi-step reaction with 8 steps

1: methanol; sodium tetrahydroborate / 2 h / 20 °C

2: triethylamine / dichloromethane / 2 h / 20 °C

3: N,N-dimethyl-formamide / 2 h / 80 °C

4: hydrogenchloride / water / 1 h / Reflux

5: methanol; sodium tetrahydroborate / 2 h / 20 °C

6: triethylamine / dichloromethane / 2 h / 20 °C

7: methanol / 2 h / 20 °C

8: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1544740-27-3
(E)-3-(4-bromo-3,5-dimethylphenyl)acrylic acid ethyl ester

: 1544740-35-3
2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene

Guidance literature:: Multi-step reaction with 9 steps

1: palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 20 °C

2: methanol; sodium tetrahydroborate / 2 h / 20 °C

3: triethylamine / dichloromethane / 2 h / 20 °C

4: N,N-dimethyl-formamide / 2 h / 80 °C

5: hydrogenchloride / water / 1 h / Reflux

6: methanol; sodium tetrahydroborate / 2 h / 20 °C

7: triethylamine / dichloromethane / 2 h / 20 °C

8: methanol / 2 h / 20 °C

9: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; palladium on activated charcoal; hydrogen; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 400822-47-1
4-bromo-3,5-dimethylbenzaldehyde

: 1544740-35-3
2-bromo-1,3-dimethyl-5-(4-(methylsulfonyl)butyl)benzene

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: palladium on activated charcoal; hydrogen / tetrahydrofuran / 1 h / 20 °C

3.1: methanol; sodium tetrahydroborate / 2 h / 20 °C

4.1: triethylamine / dichloromethane / 2 h / 20 °C

5.1: N,N-dimethyl-formamide / 2 h / 80 °C

6.1: hydrogenchloride / water / 1 h / Reflux

7.1: methanol; sodium tetrahydroborate / 2 h / 20 °C

8.1: triethylamine / dichloromethane / 2 h / 20 °C

9.1: methanol / 2 h / 20 °C

10.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; palladium on activated charcoal; hydrogen; sodium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;