2-chloro-5-nitropyrimidine

Base Information

Chemical Name:2-chloro-5-nitropyrimidine
CAS No.:400822-47-1
Molecular Formula:C9H9BrO
Molecular Weight:213.074
Hs Code.:2913000090
Mol file:400822-47-1.mol

Synonyms:4-Bromo-3,5-dimethylbenzaldehyde;

Suppliers and Price of 2-chloro-5-nitropyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-3,5-dimethylbenzaldehyde
100mg
$ 75.00

Labseeker
4-BROMO-3,5-DIMETHYLBENZALDEHYDE 98.5
10g
$ 615.00

Chemenu
4-bromo-3,5-dimethylbenzaldehyde 95+%
5g
$ 421.00

Chemenu
4-bromo-3,5-dimethylbenzaldehyde 95+%
1g
$ 173.00

Biosynth Carbosynth
4-Bromo-3,5-dimethylbenzaldehyde
1 g
$ 132.50

Biosynth Carbosynth
4-Bromo-3,5-dimethylbenzaldehyde
500 mg
$ 100.00

Biosynth Carbosynth
4-Bromo-3,5-dimethylbenzaldehyde
250 mg
$ 62.50

Biosynth Carbosynth
4-Bromo-3,5-dimethylbenzaldehyde
2 g
$ 220.00

AOBChem
4-Bromo-3,5-dimethylbenzaldehyde 97%
10g
$ 376.00

AOBChem
4-Bromo-3,5-dimethylbenzaldehyde 97%
5g
$ 221.00

Total 25 raw suppliers

Chemical Property of 2-chloro-5-nitropyrimidine

Chemical Property:

Vapor Pressure:0.004mmHg at 25°C
Refractive Index:1.587
Boiling Point:279.576°C at 760 mmHg
Flash Point:85.701°C
PSA：17.07000
Density:1.422g/cm³
LogP:2.87840
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

85% (contains <5%H2O) ^*data from raw suppliers

4-Bromo-3,5-dimethylbenzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-chloro-5-nitropyrimidine

There total 4 articles about 2-chloro-5-nitropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 100189-84-2
2,5-dibromo-1,3-dimethylbenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 400822-47-1
4-bromo-3,5-dimethylbenzaldehyde

Guidance literature:: 2,5-dibromo-1,3-dimethylbenzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.75h;

N,N-dimethyl-formamide; In diethyl ether; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1002/1099-0690(200110)2001:20<3819::AID-EJOC3819>3.0.CO;2-W

Reference yield: 10.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 27006-02-6
(4-bromo-3,5-dimethylphenyl)methanol

: 400822-47-1
4-bromo-3,5-dimethylbenzaldehyde

Guidance literature:: With lead dioxide; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 40h;
DOI:10.1134/S1070428018030053

Reference yield:

: 75344-77-3
4-bromo-3,5-dimethyl benzonitrile

: 400822-47-1
4-bromo-3,5-dimethylbenzaldehyde

Guidance literature:: 4-bromo-3,5-dimethyl benzonitrile; With diisobutylaluminium hydride; In dichloromethane; at -62 - 20 ℃; for 2h;

With hydrogenchloride; water; In dichloromethane; Reflux; Micellar solution;