[μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III)

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Chemical Name:[μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III)
CAS No.:429686-99-7
Molecular Formula:C₄₁H₄₄FeO₂PTi
Molecular Weight:703.5
Hs Code.:

[μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III)

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Chemical Property of [μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III)

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Technology Process of [μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III)

There total 1 articles about [μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 173346-69-5
1′-(diphenylphosphino)ferrocene-1-carboxylic acid

: [(η(5)-C5Me4H)2Ti(η(2)-bis(trimethylsilyl)ethyne)]

: 429686-99-7
[μ-1κ2-O,O':2(η5)-cyclopentadienylcarboxylato][2(η5)-diphenylphosphinocyclopentadienyl]bis[1,1(η5)-tetramethylcyclopentadienyl]iron(II)titanium(III)

Guidance literature:: In toluene; on vac. line; soln. of Fe(C5H4P(C6H5)2)(C5H4COOH) in toluene added to solid Ti(C5H(CH3)4)2((CH3)3SiCCSi(CH3)3); mixt. heated to 333 K for 1 h; volatiles removed under vac.; residue extd. with hexane; crystn. after concn. of extracts and storing at 273 K overnight; further crystals from mother liquor after concn. and storing;
DOI:10.1107/S0108270101019370