H₂ClB*dppm

Base Information

Chemical Name:H₂ClB*dppm
CAS No.:858355-09-6
Molecular Formula:C₂₅H₂₄BClP₂
Molecular Weight:432.677
Hs Code.:

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Chemical Property of H₂ClB*dppm

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Technology Process of H₂ClB*dppm

There total 1 articles about H₂ClB*dppm which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 63348-81-2
monochloroborane dimethyl sulfide complex

: 2071-20-7
bis-diphenylphosphinomethane

: 858355-09-6
H₂ClB*dppm

Guidance literature:: In toluene; under Ar atm. Me2S*BH2Cl was added to soln. dppm in toluene and stirred for 1 h; soln. was concd. and layered with hexane, 3 days at -30°C; elem. anal.;
DOI:10.1016/j.jorganchem.2005.01.048

Reference yield: 95.0%

: 858355-09-6
H₂ClB*dppm

: 858355-10-9
[RuCp*(NCMe)3][B(3,5-(CF₃)2C₆H₃)4]

: [RuCp*(η2-H2ClB*dppm)][B(3,5-(CF3)2C6H3)4]

Guidance literature:: In dichloromethane; under Ar atm. Ru complex and H2ClB*dppm in CH2Cl2 were stirred at room temp. for 30 min; solvent was removed in vacuo, residue was dissolved in CH2Cl2 and layered with pentane; elem. anal.;
DOI:10.1016/j.jorganchem.2005.01.048