bis[N-(3-tert-butylsalicylidene)-2,4,6-trifluororanilinato]titanium(IV) dichloride

Base Information

• Chemical Name: bis[N-(3-tert-butylsalicylidene)-2,4,6-trifluororanilinato]titanium(IV) dichloride
• CAS No.: 352033-77-3
• Molecular Formula: C₃₄H₃₀Cl₂F₆N₂O₂Ti
• Molecular Weight: 731.401

Synonyms:

Chemical Property of bis[N-(3-tert-butylsalicylidene)-2,4,6-trifluororanilinato]titanium(IV) dichloride

Chemical Property:

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Technology Process of bis[N-(3-tert-butylsalicylidene)-2,4,6-trifluororanilinato]titanium(IV) dichloride

There total 1 articles about bis[N-(3-tert-butylsalicylidene)-2,4,6-trifluororanilinato]titanium(IV) dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3-tert-butylsalicylidene)-2,4,6-trifluororaniline + titanium tetrachloride (7550-45-0) → bis[N-(3-tert-butylsalicylidene)-2,4,6-trifluororanilinato]titanium(IV) dichloride (352033-77-3)

Guidance literature:

With n-butyllithium; In diethyl ether; hexane; n-heptane; under Ar using Schlenk techniques; to org. ligand in Et2O at -78°C added n-BuLi in n-hexane over 10 min; soln. warmed to room temp.; stirred for 2 h; soln. added to n-heptane soln. of TiCl4 in Et2O at -78°C; stirred for 18 h at room temp.; concd. (vac.); CH2Cl2 added; mixt. stirred for 15 min; filtered; residuewashed (CH2Cl2); combined org. filtrates concd. in vac.; Et2O, n-hexane added; mixt. stirred for 90 min; filtered; solid washed (n-hexane); dri ed (vac.); elem. anal.;

DOI:10.1021/ja0117581

upstream raw materials:

titanium tetrachloride

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