5,15-bis(imidazolyl-4-yl)porphinatozinc

Base Information

• Chemical Name: 5,15-bis(imidazolyl-4-yl)porphinatozinc
• CAS No.: 313652-82-3
• Molecular Formula: C₁₂₄H₁₄₄N₁₆O₄Zn₂
• Molecular Weight: 2053.39
• Mol file: 313652-82-3.mol

Synonyms:

Chemical Property of 5,15-bis(imidazolyl-4-yl)porphinatozinc

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,15-bis(imidazolyl-4-yl)porphinatozinc

There total 1 articles about 5,15-bis(imidazolyl-4-yl)porphinatozinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

C4(C4H2N)2(C4H2NH)2(C3H2N2H)2(C6H4OC12H25)2 + zinc diacetate (557-34-6) → 5,15-bis(imidazolyl-4-yl)porphinatozinc (313652-82-3)

Guidance literature:

In methanol; chloroform; into a soln. of a ligand (5.2E-6 mol) in CHCl3, a soln. of Zn-contg. compd. (520E-6 mol) in MeOH was added; the soln. was refluxed for 1.5 h; the solvents were removed; the residue was dissolved in CHCl3 and washedwith distd. water; the CHCl3 layer was concd. to dryness; purifn. by si lica gel chromy. (CHCl3:CH3OH 5:1 v/v);

DOI:10.1039/b211839d

upstream raw materials:

zinc diacetate