5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene

Base Information

Chemical Name:5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene
CAS No.:1058708-15-8
Molecular Formula:C₁₇H₂₁BOSi
Molecular Weight:280.25
Hs Code.:

Synonyms:

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Chemical Property of 5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene

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Technology Process of 5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene

There total 4 articles about 5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 936499-83-1
o-[(dimesitylboryl)phenyl]dimethylsilane

: 1058708-16-9
o-(hydroxydimethylsilyl)(dimesitylboryl)benzene

: 1058708-15-8
5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene

: 1058708-14-7
[o-(dimesitylboryl)phenyl]dimethyldisiloxane

Guidance literature:: In toluene; Irradiation (UV/VIS); soln. of Fe2 complex in toluene treated with triisopropylphosphine, mixt. photolyzed for 24 h; evapd. under vac., extd. with CH2Cl2, extract concd., pptd. by addn. of hexane; elem. anal.;
DOI:10.1021/ic8007552

Reference yield: 64.0%

: 1058708-16-9
o-(hydroxydimethylsilyl)(dimesitylboryl)benzene

: 1058708-15-8
5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene

: 1058708-14-7
[o-(dimesitylboryl)phenyl]dimethyldisiloxane

Guidance literature:: In tetrahydrofuran-d8; byproducts: mesitylene; (N2); soln. of B compd. in THF-d8 was stirred at room temp. for 240 h; solvent removed (vac.); dild. with hexane; stirred for 5 min; evapd. (vac.); washed (CH3CN) with stirring; filtered; washed (CH3CN); filtrate concd. (vac.); distd. (240-250°C/0.3 mmHg); elem. anal.;
DOI:10.1021/om8004405

Reference yield: 10.0%

: 936499-83-1
o-[(dimesitylboryl)phenyl]dimethylsilane

: 75-65-0
tert-butyl alcohol

: o-(dimesitylboryl)[(tert-butoxy)dimethylsilyl]benzene

: 1058708-15-8
5,5-dimesityl-2,2-dimethyl-3,4-benzo-1,2,5-oxasilaboracyclopentene

: 1058708-14-7
[o-(dimesitylboryl)phenyl]dimethyldisiloxane

Guidance literature:: In tetrahydrofuran; (N2); mixt. of B compd. and t-BuOH in THF was stirred at room temp. for 42 h; solvent removed (vac.); dild. with hexane; stirred for 5 min; dried (vac.); dissolved in C6D6; solvent removed (vac.); washed with stirring (CH3CN); filtered; washed (CH3CN); chromd. (hexane/CH2Cl2, 5/1); elem. anal.;
DOI:10.1021/om8004405