C₃₅H₂₇BF₂N₄O

Base Information

• Chemical Name: C₃₅H₂₇BF₂N₄O
• CAS No.: 1325234-19-2
• Molecular Formula: C₃₅H₂₇BF₂N₄O
• Molecular Weight: 568.433
• Mol file: 1325234-19-2.mol

Synonyms:

Chemical Property of C₃₅H₂₇BF₂N₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₂₇BF₂N₄O

There total 2 articles about C₃₅H₂₇BF₂N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ4,5λ4-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine (1031443-55-6) → C35H27BF2N4O (1325234-19-2)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / benzene / 60 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / benzene / 60 °C

3: aluminum oxide / dichloromethane / Reflux

With aluminum oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In dichloromethane; benzene; 1: Sonogashira coupling / 2: Sonogashira coupling / 3: Knoevenagel condensation;

DOI:10.1016/j.tetlet.2011.07.028

Reference yield:

4-methoxyphenylacetylen (768-60-5) → C35H27BF2N4O (1325234-19-2)

Guidance literature:

Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / benzene / 60 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / benzene / 60 °C

3: aluminum oxide / dichloromethane / Reflux

With aluminum oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In dichloromethane; benzene; 1: Sonogashira coupling / 2: Sonogashira coupling / 3: Knoevenagel condensation;

DOI:10.1016/j.tetlet.2011.07.028

upstream raw materials:

5,5-difluoro-2,8-diiodo-1,3,7,9,10-pentamethyl-5H-4λ⁴,5λ⁴-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinine

4-methoxyphenylacetylen