Technology Process of C22H23N5O4
There total 3 articles about C22H23N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C15H17N5O4;
With
potassium hexamethylsilazane;
In
tetrahydrofuran; toluene;
at -78 ℃;
for 0.5h;
Inert atmosphere;
benzyl bromide;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
at -40 ℃;
for 3h;
Inert atmosphere;
DOI:10.1002/chem.201200457
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere
2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere
2.2: 3 h / -40 °C / Inert atmosphere
With
potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylsilane / dichloromethane / 2 h / 20 °C / Inert atmosphere
2.1: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 5 h / 20 °C / Inert atmosphere
3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere
3.2: 3 h / -40 °C / Inert atmosphere
With
triethylsilane; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol; toluene;
DOI:10.1002/chem.201200457
